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Exercises 1 The reproducibility of a method for the determination of selenium in foods was investigated by taking nine samples from a single batch of brown rice and determining the selenium concentration in each. , García-Moreno, C. and Mariné-Font, A. 1983. Analyst 108: 505) Calculate the mean, standard deviation and relative standard deviation of these results. 15 Calculate (i) the 95% and (ii) the 99% confidence limits for the true pH. , Stockwell, P. and Corns, W. 1999. Analyst 124: 185) Calculate the mean, standard deviation, relative standard deviation and 99% confidence limits of the mean.

C. and Zünd, R. E. 2000. Statistical Methods in Analytical Chemistry, 2nd edn, Wiley-Interscience, New York. ) Middleton, M. R. 2003. Data Analysis Using Microsoft Excel® Updated for Office XP, Duxbury Press, Belmont, CA, USA. (Extensive coverage of the use of Excel® for a range of scientific calculations: clearly explained examples with many screenshots. ) Minitab Statguide, Version 14. 2003. , State College, PA, USA. ) Mullins, E. 2003. Statistics for the Quality Control Chemistry Laboratory, Royal Society of Chemistry, Cambridge.

0332 ml respectively, giving quantitative confirmation of the assessments of precision made in Chapter 1. In practice, it is most unusual to make these calculations on paper. All except the most basic pocket calculators will give the results if the values of xi are keyed in. However, care must be taken that the correct key is pressed to obtain the standard deviation. e. (n − 1), replaced by n. ) Obviously, for large values of n the difference is negligible. Alternatively, readily available computer software can be used to perform these calculations (see Chapter 1).

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A two-stage model for multiple time series data of counts (2002)(en)(12s) by Berhane K., Thomas D. C.


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